Organic Syntheses, Collective Volume 9,9780471242482

Organic Syntheses, Collective Volume 9

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Edition: 1st
ISBN13: 9780471242482
ISBN10: 0471242489
Format: Hardcover
Pub. Date: 1998-03-27
Publisher(s): Wiley
List Price: $363.67

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Summary

Reflecting the increased pace of research and the many recent advances in organic chemistry, this series serves as a single-source compendium of the most up-to-date and significant procedures currently in use. Volume 9 consists of checked procedures previously published in annual volumes, revised and updated.

Author Biography

Jeremiah P. Freeman is the editor of Organic Syntheses, Collective Volume 9, published by Wiley.

Table of Contents

SYNTHESIS OF 2-SUBSTITUTED NAPHTHALENEDIOL DERIVATIVES USING CHROMIUM CARBENE COMPLEXES: 1-ACETOXY-2-BUTYL-4-METHOXYNAPHTHALENE
1
STEREOCONTROLLED PREPARATION OF 3-ACYLTERAHYDROFURANS FROM ACID-PROMOTED REARRANGEMENTS OF ALLYLIC KETALS: (2S, 3S)-3-ACETYL-8-CARBOETHOXY-2, 3-DIMETHYL-1-OXA-8-AZASPIRO[4,5]DECANE
4
HIGHLY REACTIVE CALCIUM FOR THE PREPARATION OF ORGANOCALCIUM REAGENTS: PREPARATION OF 1-ADAMANTYLCALCIUM HALIDES AND THEIR ADDITION TO KETONES: 1-(1-ADAMANTYL) CYCLOHEXANOL
9
(3S,4S)-3-AMINO-1-(3,4-DIMETHOXYBENZYL)-4-[(R)-2,2-DIMETHYL-1,3-DIOXOLAN-4-YL]-2-AZETIDINONE
13
ENANTIOMERICALLY PURE Beta-AMINO ACIDS FROM 2-tert-BUTYL-1-CARBOMETHOXY-2, 3-DIHYDRO-4(1H)-PYRIMIDINONE: (R)-3-AMINO-3-(p-METHOXYPHENYL) PROPIONIC ACID
17
(S)-3-AMINO-2-OXETANONE p-TOLUENESULFONIC ACID SALT
24
FLASH VACUUM PYROLYSIS: BENZOCYCLOBUTENONE
28
4-BENZYL-10, 19-DIETHYL-4, 10, 19-TRIAZA-1, 7, 13, 16-TETRAOXACYCLOHENEICOSANE (TRIAZA-21-CROWN-7)
34
(-)-2-O-BENZYL-L-GLYCERALDEHYDE
39
(E)-1-BENZYL-L-3-(1-IODOETHYLIDENE) PIPERIDINE: NUCLEOPHILE-PROMOTED ALKYNE-IMINIUM ION CYCLIZATIONS
46
DIASTEREOSELECTIVE HOMOLOGATION OF D-(R)-GLYCERALDEHYDE ACETONIDE USING 2-(TRIMETHYLSILYL) THIAZOLE: 2-O-BENZYL-3,4-ISOPROPYLIDENE-D-ERYTHROSE
52
SYNTHESIS OF N-PROTECTED XXX-AMINO ACIDS FROM N-(BENZYLOXYCARBONYL)-L-SERINE VIA ITS Beta-LACTONE: N(XXX)-(BENZYLOXYCARBONYL)-Beta-(PYRAZOL-1-YL)-L-ALANINE
58
N-(BENZYLOXYCARBONYL)-L-SERINE Beta-LACTONE
58
N-(BENZYLOXYCARBONYL)-L-VINYLGLYCINE METHYL ESTER
63
ENANTIOSELECTIVE, CATALYTIC DIELS-ALDER REACTION: (1S-ENDO)-3-(BICYCLO [2.2.1]HEPT-5-EN-2-YLCARBONYL)-2-OXAZOLIDINONE
67
2.2'-BI-5, 6-DIHYDRO-1,3-DITHIOLO [4, 5-b][1, 4]-DITHINYLIDENE (BEDT-TTF)
72
(S)-(-)- AND (R)-(+)-1,1'-BI-2-NAPHTHOL
77
2.3-BIS(PHENYLSULFONYL-1,3-BUTADIENE
82
BIS(TRIFLUOROETHYL)(CARBOETHOXYMETHYL)PHOSPHONATE
88
BIS(TRIMETHYLSILYL) PEROXIDE (BTMSPO)
91
9-BORABICYCLO[3.3.1]NONANE DIMER
95
5-(4-BROMOBENZOYL-2-(4-MORPHOLINO)-3-PHENYLTHIOPHENE
99
9-BROMO-9-PHENYLFLUORENE
103
1-BROMO-1-PHENYLTHIOETHENE
107
AN AMBIPHILIC DIENE FOR DIELS-ALDER CYCLOADDITIONS: 3-BROMO-2H-PYRAN-2-ONE
112
SYNTHESIS OF FUNCTIONALIZED ENZYNES BY PALLADIUM/COPPER-CATALYZED COUPLING REACTIONS OF ACETYLENES WITH (Z)-2, 3-DIBROMOPROPENOIC ACID ETHYL ESTER: (Z)-2-BROMO-5-(TRIMETHYLSILYL)-2-PENTEN-4-YNOIC ACID ETHYL ESTER
117
N-tert-BUTOXYCARBONYL-2-BROMOPYRROLE
121
l-(tert-BUTOXYCARBONYL)INDOLINE
124
N-tert-BUTOXYCARBONYL-L-SERINE Beta-LACTONE
24
2-SUBSTITUTED PYRROLES FROM N-tert-BUTOXYCARBONYL-2-BROMOPYRROLE: N-tert-BUTOXYCARBONYL-2-TRIMETHYLSILYPYRROLE
121
tert-BUTYL 3-BROMOPROPIOLATE
129
2-tert-BUTYL-1-CARBOMETHOXY-2, 3-DIHYDRO-4(1H)-PYRIMIDINONE
17
(4R)-(+)-tert-BUTYLDIMETHYLSILOXY-2-CYCLOPENTEN-1-ONE
132
(4S)-(-)-tert-BUTYLDIMETHYLSILOXY-2-CYCLOPENTEN-1-ONE
136
3-(S)-[(tert-BUTYLDIPHENYLSILYL)OXY]-2-BUTANONE
139
ALLYLIC ALCOHOLS BY ALKENE TRANSFER FROM ZIRCONIUM TO ZINC: 1-[(tert-BUTYLDIPHENYLSILYL)OXY]-DEC-3-EN-5-OL
143
2-tert-BUTYL-1, 1, 3, 3-TETRAMETHYLGUANIDINE
147
(-)-(1S,4R)-CAMPHANOYL CHLORIDE
151
RHODIUM-CATALYZED HETEROCYCLOADDITION OF A DIAZOMALONATE AND A NITRILE: 4-CARBOMETHOXY-5-METHOXY-2-PHENYL-1, 3-OXAZOLE
155
CHLOROBIS(XXX(5)-CYCLOPENTADIENYL)HYDRIDOZIRCONIUM (SCHWARTZ'S REAGENT)
162
PYRIDINE-DERIVED TRIFLATING REAGENTS: N-(5-CHLORO-2-PYRIDYL)TRIFLIMIDE
165
ASYMMETRIC HYDROGENATION OF ALLYLIC ALCOHOLS USING BINAP-RUTHENIUM COMPLEXES: (S)-(-)-CITRONELLOL
169
A STABLE CHIRAL 1, 4-DIHYDROPYRIDINE EQUIVALENT FOR THE ASYMMETRIC SYNTHESIS OF SUBSTITUTED PIPERIDINES: 2-CYANO-6-PHENYLOXAZOLOPIPERIDINE
176
BENZOANNELATION OF KETONES: 3, 4-CYCLODODECENO-1-METHYLBENZENE
180
2-CYCLOHEXENE-1, 4-DIONE
186
PALLADIUM(0)-CATALYZED REACTION OF 9-ALKYL-9-BORABICYCLO[3.3.1]NONANE WITH 1-BROMO-1-PHENYLTHIOETHENE: 4-(3-CYCLOHEXENYL)-2-PHENYLTHIO-1-BUTENE
107
1, 3, 5-CYCLOOCTATRIENE
191
CONVERSION OF AMINES TO PHOSPHO ESTERS: DECYL DIETHYL PHOSPHATE
194
DETRIFLUOROACETYLATIVE DIAZO GROUP TRANSFER: (E)-1-DIAZO-4-PHENYL-3-BUTEN-2-ONE
197
4, 5-DIBENZOYL-1, 3-DITHIOLE-1-THIONE
203
2, 3-DIBROMO-1-(PHENYLSULFONYL)-1-PROPENE
207
(+)-(2R, 8aR(*))-[(8, 8-DICHLOROCAMPHORYL)SULFONYL]OXAZIRIDINE
212
DIETHYL (2S, 3R)-2-(N-tert-BUTOXYCARBONYL)AMINO-3-HYDROXYSUCCINATE
220
PREPARATION AND USE IN THE SYNTHESIS OF ALKYNES: DIETHYL (DICHLOROMETHYL) PHOSPHONATE
230
SYNTHESIS OF AN XXX-HYDROXYAMIDE: GENERATION OF N, N-DIETHYLCARBAMOYLLITHIUM VIA LITHIUM-TELLURIUM EXCHANGE: N, N-DIETHYL-2-HHYDROXY-4-PHENYLBUTANAMIDE
234
DIETHYL 1-PROPYL-2-OXOETHYLPHOSPHONATE
239
3, 4-DIETHYLPYRROLE
242
(3, 3-DIFLUOROALLYL)TRIMETHYLSILANE
247
3-[(1S)-1, 2-DIHYDROXYETHYL]-1, 5-DIHYDRO-3H-2, 4-BENZODIOXEPINE
251
(+)-(2R, 8aR*)-[(8,8-DIMETHOXYCAPHORYL)SULFONYL]OXAZIRIDINE
212
2,2'-DIMETHOXY-6-FORMYLBIPHENYL
258
5,7-DIMETHOXY-3-METHYLINDAZOLE
264
TETRAHYDRO-3-BENZAZEPIN-2-ONES: LEAD TETRAACETATE OXIDATION OF ISOQUINOLINE ENAMIDES: 7, 8-DIMETHOXY-1, 3, 4, 5-TETRAHYDRO-2H-3-BENZAZEPIN-2-ONE
268
PREPARATION OF BICYCLO[3.2.0]HEPT-3-EN-6-ONES: 1, 4-DIMETHYBICYCLO[3.2.0]HEPT-3-EN-6-ONE
275
(1XXX, 2XXX, 6Beta)- AND (1XXX, 2Beta, 6XXX)-2, 6-DIMETHYLCYCLOHEXANECARBONITRILE
281
DIMETHYLDIOXIRANE
288
SYNTHESIS OF Beta-LACTONES AND ALKENES VIA THIOL ESTERS: (E)-2, 3-DIMETHYL-3-DODECENE
293
A USEFUL SERINAL DERIVATIVE: 1, 1-DIMETHYLETHYL (S)- OR (R)-4-FORMYL-2, 2-DIMETHYL-3-OXAZOLIDINECARBOXYLATE
300
1, 3-DIOLS FROM LITHIUM Beta-LITHIOALKOXIDES GENERATED BY THE REDUCTIVE LITHIATION OF EPOXIDES: 2, 5-DIMETHYL-2, 4-HEXANEDIOL
306
DIASTEREOSELECTIVE FORMATION OF trans-1, 2-DISUBSTITUTED CYCLOHEXANES FROM ALKYLIDENEMALONATES BY AN INTRAMOLECULAR ENE REACTION: DIMETHYL (1'R, 2'R, 5'R)-2-(2'-ISOPROPENYL-5'-METHYLCYCLOHEX-1'-YL)-PROPANE-1, 3-DIOATE
310
DIALKYL MESOXALATES BY OZONOLYSIS OF DIALKYL BENZALMALONATES: DIMETHYL MESOXALATE
314
REGIO- AND STEREOSELECTIVE CARBOXYLATION OF ALLYLIC BARIUM REAGENTS: (E)-4, 8-DIMETHYL-3, 7-NONADIENOIC ACID
317
HIGHLY ENANTIOSELECTIVE INTRAMOLECULAR CYCLOPROPANATION CATALYZED BY DIRHODIUM (II) TETRAKIS[METHYL 2-PYRROLIDONE-5(R)-CARBOXYLATE]: (1R, 5S)-(-)-6, 6-DIMETHYL-3-OXABICYCLO[3.1.0]HEXAN-2-ONE
322
MANGANESE-COPPER-CATALYZED CONJUGATE ADDITION OF ORGANOMAGNESIUM REAGENTS TO XXX, Beta-ETHYLENIC KETONES: 2-(1, 1-DIMETHYLPENTYL)-5-METHYL CYCLOHEXANONE
328
PREPARATION AND DIELS-ALDER REACTION OF A REACTIVE, ELECTRON-DEFICIENT HETEROCYCLIC AZADIENE: 1, 2-DIAZINE AND PYRROLE INTRODUCTION: DIMETHYL 4-PHENYL-1, 2-DIAZINE-3, 6-DICARBOXYLATE
335
(S)-DIMETHYL N-(9-PHENYLFLUOREN-9-YL)ASPARTATE
344
PREPARATION AND DIELS-ALDER REACTION OF A REACTIVE, ELECTRON-DEFICIENT HETEROCYCLIC AZADIENE: 1, 2-DIAZINE AND PYRROLE INTRODUCTION: DIMETHYL 3-PHENYLPYRROLE-2, 5-DICARBOXYLATE
335
SPIROANNELATION VIA ORGANOBIS(CUPRATES): 9, 9-DIMETHYLSPIRO[4.5]DECAN-7-ONE
350
DIMETHYL 1, 2, 4, 5-TETRAZINE-3, 6-DICARBOXYLATE
335
REARRANGEMENT OF trans-STILBENE OXIDE TO DIPHENYLACETALDEHYDE WITH CATALYTIC METHYLALUMINUM BIS(4-BROMO-2, 6-Dl-tert-BUTYLPHENOXIDE): DIPHENYL ACETALDEHYDE
356
(R)-(-)-2, 2-DIPHENYLCYCLOPENTANOL
362
CYCLOPROPANATION USING AN IRON-CONTAINING METHYLENE TRANSFER REAGENT: 1, 1-DIPHENYLCYCLOPROPANE
372
(R, R)-1, 2-DIPHENYL-1, 2-ETHANEDIOL
383
(1R, 2R)-(+)- AND (1S, 2S)-(-)-1, 2-DIPHENYL-1, 2-ETHYLENEDIAMINE
387
(R)-(+)-2-(DIPHENYLHYDROXYMETHYL)PYRROLIDINE
391
INVERSE ELECTRON-DEMAND DIELS-ALDER CYCLOADDITION OF A KETENE DITHIOACETAL COPPER HYDRIDE-PROMOTED REDUCTION OF A CONJUGATED ENONE: 9-DITHIOLANOBICYCLO[3.2.2]NON-6-EN-2-ONE
396
4-DODECYLBENZENESULFONYL AZIDES
400
ALKYLIDENATION OF ESTER CARBONYL GROUPS: (Z)-1-ETHOXY-1-PHENYL-1-HEXENE
404
ETHYL (R, E)-4-O-BENZYL-4, 5-DIHYDROXY-2-PENTENOATE
39
ETHYL (Z)-3-BROMO-2-PROPENOATE
415
ETHYL (Z)-2, 3-DIBROMOPROPENOATE
117
REGIOSELECTIVE SYNTHESIS OF 3-SUBSTITUTED INDOLES: 3-ETHYLINDOLE
417
ETHYL 2-METHYL-5-PHENYL-3-FURANCARBOXYLATE
422
ESTER HOMOLOGATION VIA YNOLATE ANIONS: ETHYL 1-NAPHTHYLACETATE
426
ETHYL 3-OXO-4-PENTENOATE (NAZAROV'S REAGENT)
432
XXX-ACETYLENIC ESTERS FROM XXX-ACYLMETHYLENEPHOSPHORANES: ETHYL 4, 4, 4-TRIFLUORO TETROLATE
436
CONVERSION OF METHYL KETONES INTO TERMINAL ACETYLENES: ETHYNYLFERROCENE
411
STEREOSELECTIVE SYNTHESIS OF 2, 2-DISUBSTITUTED 1-FLUOROALKENES: (Z)-[2-(FLUORO METHYLENE)CYCLOHEXYL]BENZENE
442
REACTION OF SULFOXIDES WITH DIETHYLAMINOSULFUR TRIFLUORIDE. A REAGENT FOR THE SYNTHESIS OF FLUOROALKENES: FLUOROMETHYL PHENYL SULFONE
446
(E)-[[FLUORO-(2-PHENYLCYCLOHEXYLIDENE)METHYL]SULFONYL]BENZENE
442
D-(R)-GLYCERALDEHYDE ACETONIDE
450
L-(S)-GLYCERALDEHYDE ACETONIDE
454
CHIRAL BICYCLIC LACTAMS AS TEMPLATES FOR PYRROLIDINES AND PYRROLIDINONES: S-(-)-5-HEPTYL-2-PYRROLIDINONE
457
A SELECTIVE, HETEROGENEOUS OXIDATION USING A MIXTURE OF POTASSIUM PERMANGANATE AND CUPRIC SULFATE: (3aS, 7aR)-HEXAHYDRO)-(3S, 6R)-DIMETHYL-2(3H)-BENZOFURANONE
462
CYCLOPENTANONE ANNULATION VIA CYCLOPROPANONE DERIVATIVES: (3aBeta, 9bBeta)-1, 2, 3a, 4, 5, 9b-HEXAHYDRO-9b-HYDROXY-3a-METHYL-3H-BENZ[e]INDEN-3-ONE
466
PREPARATION AND REACTIONS OF ALKENYLCHROMIUM REAGENTS: 2-HEXYL-5-PHENYL-1-PENTEN-3-OL
472
ALKYNYL(PHENYL)IODONIUM TOSYLATES: PREPARATION AND STEREOSPECIFIC COUPLING WITH VINYLCOPPER REAGENTS. FORMATION OF CONJUGATED ENYNES: 1-HEXYNYL(PHENYL) IODONIUM TOSYLATE
477
DIRECT DEGRADATION OF THE BIOPOLYMER POLY[(R)-3-HYDROXYBUTYRIC ACID]: (R)-3-HYDROXYBUTANOIC ACID AND ITS METHYL ESTER
483
ENANTIOSELECTIVE HYDROLYSIS OF cis-3, 5-DIACETOXYCYCLOPENTENE: (1R, 4S)-(+)-4-HYDROXY-2-CYCLOPENTENYL ACETATE
487
PREPARATION AND USE OF (METHOXYMETHOXY)METHYLLITHIUM: 1-(HYDROXYMETHYL) CYCLOHEPTANOL
493
STEREOSELECTIVE ALDOL REACTION OF DOUBLY DEPROTONATED 2-HYDROXY-1, 2, 2-TRIPHENYLETHYL ACETATE(HYTRA): (R)-3-HYDROXY-4-METHYLPENTANOIC ACID
497
1, 2-ADDITION OF A FUNCTIONALIZED ZINC-COPPER ORGANOMETALLIC [RCu(CN)Znl] TO AN XXX, Beta-UNSATURATED ALDEHYDE: (E)-2-(4-HYDROXY-6-PHENYL-5-HEXENYL)-1H-ISOINDOLE-1, 3(2H)-DIONE
502
(R)-(+)-2-HYDROXY-1, 2, 2-TRIPHENYLETHYL ACETATE (HYTRA)
507
SYNTHESIS OF 7-SUBSTITUTED INDOLINES VIA DIRECTED LITHIATION OF 1-(tert-BUTOXYCARBONYL)INDOLINE: 7-INDOLINECARBOXALDEHYDE
124
(Z)-Beta-IODOACROLEIN
510
8-EXO-IODO-2-AZABICYCLO[3.3.0]OCTAN-3-ONE
516
(Z)- AND (E)-1-IODOHEPT-1-EN-E-OL
510
A SIMPLE AND CONVENIENT METHOD FOR THE OXIDATION OF ORGANOBORANES USING SODIUM PERBORATE: (+)-ISOPINOCAMPHEOL
522
TITANIUM-MEDIATED ADDITION OF SILYL DIENOL ETHERS TO ELECTROPHILIC GLYCINE: 4-KETOPIPECOLIC ACID HYDROCHLORIDE
526
4-KETOUNDECANOIC ACID
530
ACETYLENIC ETHERS FROM ALCOHOLS AND THEIR REDUCTION TO Z- AND E-ENOL ETHERS: (Z)- AND (E)-1-MENTHOXY-1-BUTENE
533
ACETYLENIC ETHERS FROM ALCOHOLS AND THEIR REDUCTION TO Z- AND E-ENOL ETHERS: 1-MENTHOXY-1-BUTYNE
533
MESITYLENESULFONYLHYDRAZINE
281
REGIO- AND STEREOSELECTIVE INTRAMOLECULAR HYDROSILYLATION OF XXX-HYDROXY ENOL ETHERS: 2, 3-SYN-2-METHOXYMETHOXY-1, 3-NONANEDIOL
539
(E, Z)-1-METHOXY-2-METHYL-3-(TRIMETHYLSILOXY)-1, 3-PENTADIENE
548
4-METHOXY-4'-NITROBIPHENYL
553
(4-METHOXYPHENYL)ETHYNE
230
7-METHOXYPHTHALIDE
559
METHYL 3-BROMOPROPIOLATE
129
DOUBLE HYDROXYLATION REACTION FOR CONSTRUCTION OF THE CORTICOID SIDE CHAIN: 16XXX-METHYLCORTEXOLONE
564
2-METHYL-1, 3-CYCLOPENTANEDIONE
570
METHOXYCARBONYLMETHYLATION OF ALDEHYDES VIA SILOXYCYCLOPROPANES: METHYL 3, 3-DIMETHYL-4-OXOBUTANOATE
573
STEREOSELECTIVE ALKENE SYNTHESIS VIA 1-CHLORO-1-[(DIMETHYL)PHENYLSILYL]ALKANES] AND XXX-(DIMETHYL)PHENYLSILYL KETONES: 6-METHYL-6-DODECENE
580
2-METHYLENE-1, 3-DITHIOLANE
585
ASYMMETRIC HYDROGENATION OF 3-OXO CARBOXYLATES USING BINAP-RUTHENIUM COMPLEXES: (R)-(-)-METHYL 3-HYDROXYBUTANOATE
483, 589
ASYMMETRIC CATALYTIC GLYOXYLATE-ENE REACTION: METHYL (2R)-2-HYDROXY-4-PHENYL-4-PENTENOATE
596
METHYL 5-METHOXYINDOLE-2-ACETATE
601
A GENERAL PROCEDURE FOR MITSUNOBU INVERSION OF STERICALLY HINDERED ALCOHOLS: INVERSION OF MENTHOL: (1S, 2S, 5R)-5-METHYL-2-(1-METHYLETHYL)CYCLOHEXYL 4-NITROBENZOATE
607
(R)-(-)-10-METHYL-1(9)-OCTAL-2-ONE
610
SYNTHESIS OF Beta-KETO ESTERS BY C-ACYLATION OF PREFORMED ENOLATES WITH METHYL CYANOFORMATE: METHYL (1XXX, 4aBeta, 8aXXX)-2-OXODECAHYDRO-1-NAPHTHOATE
619
2, 3-DIBROMO-1-(PHENYLSULFONYL)-1-PROPENE AS A VERSATILE REAGENT FOR THE SYNTHESIS OF FURANS AND CYCLOPENTENONES: 2-METHYL-3-[(PHENYLSULFONYL)METHYL]-2-CYCLOPENTEN-1-ONE
207
2, 3-DIBROMO-1-(PHENYLSULFONYL)-1-PROPENE AS A VERSATILE REAGENT FOR THE SYNTHESIS OF FURANS AND CYCLOPENTENONES: 2-METHYL-4-[(PHENYLSULFONYL)METHYL]-FURAN
207
A GENERAL METHOD FOR THE PREPARATION OF XXX-BRANCHED AMINO ACIDS: (S)-2-METHYL PROLINE
626
OXIDATION OF SECONDARY AMINES TO NITRONES: 6-METHYL-2, 3, 4, 5-TETRAHYDROPYRIDINE N-OXIDE
632
3-MORPHOLINO-2-PHENYLTHIOACRYLIC ACID MORPHOLIDE
99
NITROACETALDEHYDE DIETHYL ACETAL
636
2, 3, 7, 8, 12, 13, 17, 18-OCTAETHYLPORPHYRIN
242
CONJUGATE ADDITION OF A VINYLZIRCONIUM REAGENT: 3-(1-OCTEN-1-YL) CYCLOPENTANONE
640
SPIROANNELATION OF ENOL SILANES: 2-OXO-5-METHOXYSPIRO[5, 4]DECANE
643
NICKEL-CATALYZED, GEMINAL DIMETHYLATION OF ALLYLIC DITHIOACETALS: (E)-1-PHENYL-3, 3-DIMETHYL-1-BUTENE
649
(E)-5-PHENYLDODEC-5-EN-7-YNE
477
(S)-N-(9-PHENYLFLUOREN-9-YL)ALANINE
344
1-PHENYL-2, 3, 4, 5-TETRAMETHYLPHOSPHOLE
653
PHENYLTHIOACETYLENE
656
PHENYL VINYL SULFIDE
662
PYRIDINE-DERIVED TRIFLATING REAGENTS: N-(2-PYRIDYL)TRIFLIMIDE
165
3-PYRROLINE
666
SYNTHESIS OF EPOXIDES USING DIMETHYLDIOXIRANE: trans-STILBENE OXIDE
288
PREPARATION OF POLYQUINANES BY DOUBLE ADDITION OF VINYL ANIONS TO SQUARATE ESTERS: 4, 5, 6, 6a-TETRAHYDRO-3a-HYDROXY-2, 3-DIISOPROPOXY-4, 6a-DIMETHYL-1(3aH)-PENTALENONE
670
(S)-TETRAHYDRO-1-METHYL-3, 3-DIPHENYL-1H, 3H-PYRROLO[1, 2-c] [1, 3, 2]OXAZABOROLE-BORANE COMPLEX
676
SUBSTITUTION REACTIONS OF 2-BENZENESULFONYL CYCLIC ETHERS: TETRAHYDRO-2-(PHENYLETHYNYL)-2H-PYRAN
688
9-THIABICYCLO[3.3.1]NONANE-2, 6-DIONE
692
ASYMMETRIC SYNTHESIS OF trans-2-AMINOCYCLOHEXANECARBOXYLIC ACID DERIVATIVES FROM PYRROLOBENZODIAZEPINE-5, 11-DIONES: (1S, 2S)-2-(N-TOSYLAMINO) CYCLOHEXANECARBOXYLIC ACID
698
A HYDROXYMETHYL ANION EQUIVALENT: TRIBUTYL[(METHOXYMETHOXY)METHYL] STANNANE
704
TRIBUTYL(3-METHYL-2-BUTENYL)TIN
707
[3 + 2]-ANIONIC ELECTROCYCLIZATION USING 2, 3-BIS(PHENYLSULFONYL)-1, 3-BUTADIENE: trans-4, 7, 7-TRICARBOMETHOXY-2-PHENYLSULFONYLBICYCLO[3.3.0]OCT-1-ENE
82
1-TRIFLUOROMETHYL-1-CYCLOHEXANOL
711
(2S, 4S)-2, 4, 5-TRIHYDROXYPENTANOIC ACID 4, 5-ACETONIDE METHYL ESTER
717
CHIRAL (ACYLOXY)BORANE COMPLEX-CATALYZED ASYMMETRIC DIELS-ALDER REACTION: (1R)-1, 3, 4-TRIMETHYL-3-CYCLOHEXENE-1-CARBOXALDEHYDE
722
2, 2, 6-TRIMETHYLCYCLOHEXEN-1-YL IODIDE
147
NICKEL-CATALYZED SILYLOLEFINATION OF ALLYLIC DITHIOACETALS: (E, E)-TRIMETHYL (4-PHENYL-1, 3-BUTADIENYL)SILANE
727
1, 2, 3-TRIPHENYLCYCLOPROPENIUM BROMIDE
730
A WATER-SOLUBLE TIN HYDRIDE: TRIS[3-(2-METHOXYETHOXY)PROPYL]STANNANE
733
TRIS(TRIMETHYLSILYL)SILANE
738
UBIQUINONE-1
741
(1R, 5R)-(+)-VERBENONE
745
TYPE OF REACTION INDEX 749(16)
TYPE OF COMPOUND INDEX 765(18)
FORMULA INDEX 783(10)
AUTHOR INDEX 793(6)
GENERAL INDEX 799(36)
HAZARD AND WASTE DISPOSAL INDEX 835(4)
CONCORDANCE INDEX 839

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